Dmt acetone instead of naphtha. Addition of 1 g NaOH to basify 3.
Dmt acetone instead of naphtha naphtha, xylene, etc. NPS for FASA Instead of using Aceton as the DMT carrier solution, some non-polar solvents through swim's experiences, a/b generally yields less (though purer) product than STB (even after recrystallization). So it’s possible a bark extract of acetone may directly afford fumarate without using naphtha. Cheeto #41. Could I then purify the crude extract by dissolving it in warm naphtha and leaving it to freeze precipitate? Any advice is welcome :D Well, if you evaporate your naphtha to recover DMT it isn't entirely unexpected for it to form an oil. I'd like to try classic A/B Lextek for my first extraction attempt, using limonene instead of naphtha as a NPS, so I don't have to worry as much about contaminants if I screw up. Your question is open ended. What I am trying to understand is how different they are with regard to how much of a problem is it to use pure acetone instead of anhydrous acetone in the tek. Naphtha is around 4. Addition of 1 g NaOH to basify 3. Reply. Naphtha pulls a wider range of plant alkaloids from whatever root bark is being used. 6, Toluene is 2. p. Upvote 0 Downvote. Freebase DMT is many times more Hi, I've read some posts that say that DMT is highly soluble in Acetone, but I've noticed that nobody ever mentions Acetone in extraction threads or teks Which others solvents you have access to instead of naphtha? Hexane, heptane, octane, nonane, decane all will work for STB and freeze precipitation. This time I carefully prepared a stb but now I see I added acetone instead of Acetone is in the middle so it mixes with non polar and polar solvents (to a point). dmt fumarate is insoluble in acetone and very poorly soluble in IPA, whilst dmt citrate, dmt tartrate and dmt malate are quite soluble in both IPA and acetone. Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » STB » Using Limonene instead of Naphtha in STB. Based on this data, DMT is most soluble in toluene and dcm. Weigh the result and figure your yield. as for the ammonia wash. Even if that wasn't true at all. The idea of using DMT salts follows the commercial success of Juul's development of nicotine salts as explained in this thread. Thread starter young_bot; Start date Sep 7, 2009; Prev. My preferred ratio and tek is based on cybs and and fasa wash: - Add 75 g shredded DMT-Nexus, for all your information on DMT, Ayahuasca (Should SWIM use air tight mason jars instead?) 4. Sometimes a mini ab instead of re x. DMT will be more soluble Almost finished with first dmt extraction and am stuck on the last step, I've put the naphtha containing the dmt into the freezer and when I took it out the next day there was a solid frozen layer at the bottom, I'm assuming this is a mix of dmt and fats. ). So if you use acetone as your non polar solvent it will mix with the basic water and it will not And yes, there are many solvents that could potentially be used. As soon as I get all of my lab grade Sodium DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO : Options . It is a hydrocarbon, and thus non polar, and can pull dmt from a basic aqueous layer. In this case fully evaporate the solution to obtain the yield. By this approach one knows when to stop pulling since at some point Hexane, heptane octane and nonane will be more than fine. Unfortunately, acetic anhydride is a chemical that is hard to obtain (listed precursor), so a home chemist is probably left with recrystallization and chromatography. try using lab grade heptane instead of naphtha and I use a food dehydrator after I pour off the solvent and scrape the gallon jugs. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? Naphtha is the most popular solvent. Using Limonene instead of Naphtha in STB: Options . Ideas below are early development using a longer process going through DMT FB. Then, fill a large bowl with ice, sprinkle a bunch of salt on top and push the glass container with the naphtha down into the salty ice. DMT Fumarate precipitates out. DMT-Nexus, for all your information on DMT, Ayahuasca 5 pulls with 50ml naptha for each bottle. Everything went accordingly until the step where the solvent is used. I fear a lot of good DMT has been thrown away during re-X. I thought of something, being that i'm going for freebase couldn't i just do a real good acetone wash, dry, frebase, dry, and go ahead and make my 3 acetone Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » STB » Using Limonene instead of Naphtha in STB. Can you use white spirit / clean spirit instead of Heptane/Naphtha . young_bot #1. Question/Advice I was just wondering if this procedure will work for creating pure dmt crystals. What I have already found out about sodium carbonate is that one cant basify MHRB with sodium carbonate and pull it with naphtha or xylene, they would have to pull it w/ DCM. Instead of using vinegar just use hcl or citric acid. Would u try it again 4 me , but acetone and salt instead ---dont have any dmt ingredients (plants ) rn but i love your idea Reply reply DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO. It is practically insoluble in acetone. 7, Acetone is -0. Yeah I was just thinking as acetone is much less toxic them naptha, if you were too dissolve dmt in acetone, the naptha would go to the top and evaporate first (assuming there was solvent residue in the end crystals or something), then the acetone, leaving you with naptha free dmt? but from what I read heptane is a lot less toxic than DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! Visit our NEW FORUM to join the latest discussions. I was thinking maybe chloroform would be easier to get a hold of, after all you can just mix bleach and acetone. i have small (200ml bowls Plus using vinegar would make the product more edible anyway (I eat dmt). I'll use that acronym throughout this post to refer to anhydrous acetone that has been saturated with fumaric acid. Same happens with DMT and Naphtha above the DMT melting point. However, it makes sense to use acetone since it's a much quicker evaporating solvent. 6, Toluene is The DMT in mimosa is a salt, most likely DMT tannate. Posted : 1/21/2009 Can I use naphtha as a solvent when making changa instead of acetone? I only have naphtha readily available besides 70% isopropyl alcohol, which has EDIT - This thread has turned more into an acetone extraction question thread, check page 2. Safety. Put the tray in and let it sit undisturbed for 24 hours. SWIM prefers to siphon it off using something like a turkey baster, then let Trying to do an extraction Acacia following Cyb's hybrid tek. My first attempt was DMT benzoate, but it crashes from PG at room temp. Shaking this vigorously will change the freebase DMT back into salt and they will fall out of the Naphtha into the aqueous solution. STB . This advance merely opens the door for pulling real fumarate out of a DMT mixture considerably easier using acetone. They think you're suggesting using gasoline, (which is less than half octane) instead of ACS grade octane. DMT-Nexus, for all your information on Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » A/B » Sodium (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO : Options . New posts Search forums. You will generally get more lipids, fats, oils, etc from the bark when using naphtha, this will create more yellow dmt crystals (during crystallization) with some brownish goo on the bottom that some people call jungle spice or polymorphs (chains of dmt). So the long "CIELO Needles" absolutely need water to be formed and it is tightly bound inside of Hello everyone :d I've been wondering, would it be viable for someone to use Limonene instead of Naphtha in a STB tek, Lazy Man's, let's suppose? If so Forums. I can promise you that 99% of the time, if it smelled and tasted of naphtha, it's because care was not taken in fully drying out Hi, I've read some posts that say that DMT is highly soluble in Acetone, but I've noticed that nobody ever mentions Acetone in extraction threads or teks, and also nobody mentions it in the many "what can I use instead of naptha" threads; is there a reason for this or would acetone work well as DMT-Nexus, for all your information on DMT, I thought it would be a good idea to use ACRB (instead of MHRB) thinking I’d get a higher yield. solvent used instead of naphtha. A basic phase is hydroxanion-rich, and cation-poor (lacks protons), and those hydroxyanions disrupt interactions between acetone and water molecules. Will this work? Limonene's vapor pressure is a lot lower than naphtha's (0. Location: Georgia. DMT should not taste or smell like naphtha so I think it's safe to say your buddy probably didn't make a very clean product. (not necessray to remove, but some prefer to), use heptane (or naphtha, if SWIY has a taste for such things). use a more accessible container instead of jar. DMT does have a smell, but it is very different from the solvent. The DMT is now in salt form but the fats and oils are still in the Naphtha. Not sure if it happened but I remember a thread in 2018 between a dmt user and a representative for zippo confirming it’s no longer naphtha but a very similar petroleum distillate. Joined: 19-Mar-2009. Crank your freezer as cold as it can go. Migrated topic. Figure 8 shake for 1 min (instead of 30 sec, no emulsion problems occurred), 10 min rest, repeat 4 times (5 shakes in total incl initial shake). . Dissolved everything together in acetone for a DMT-Fumerate FASA conversion. Any other ligher fluid is also perfect if it pass the evaporation test (a small drip from placed on a spotlessly clean mirror evaporates without leaving any filmy white residue). Posted : 11/22/2008 3:37:21 SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Bestine would work better for a pull than not heating it up. Wiki. The dry residue is washed with naphtha and then recrystallized from boiling 99% IPA with a naphtha co-solvent addition. the logp of dmt is 2. New Dissolve 309 mg of Fumaric acid in another batch of 50 ml of Acetone. Let it sit a few hours mixing occasionally and making sure it stays wet. Submerge the jar with a lid little open I very hot water and take it out every 10min and turn it upside down so the ronsonol lighter fluid can catch all the dmt. 1:3 Ethyl Acetate: (like 1:3 EA:Naphtha). Would you not get purer/bigger crystals by recrystallizing extracted dmt in acetone? For sure, BUT: Acetone and ethanol are not heavy hydrocarbon solvents. ] Acetone is miscible with naphtha; what you have done so far will not help as the acetone will completely prevent Pitubo, can you please show me where I asked what anhydrous acetone is? I never did that. Do you just do a usual naphtha tek, and when you pull the naphtha, instead of letting the naphtha evaporate, or doing a freeze precip, you just mix vinegar with the naphtha, mix and let sit for a bit, then collect the vinegar and let the vinegar evaporate. Heptane evaporates faster and boils at a lower temperature than naphtha. Best of luck to If one doesnt have a scale or for some reason cant weigh the spice, warm up a quantity of naphtha in a shotglass without the dmt and slowly add small quantities of the warm naphtha to the container containing dmt while stiring, until most dmt dissolved but a bottom layer of goo remains. 5. Do not let the naphtha evaporate any more than half. I'll explain this logp situation, as it is relevant: the logp of dmt is 2. So if there is a substantial amount of acetate salts in the extract, then it must have been a pretty sloppy pull. Posts: 17. 3. But it will contain a lot of Acetone, which will slowly drip out. Can you use ethyl acetate instead of naphtha i can’t find it in nz Share Add a Comment. Next time anyone is chasing xtals and has a leftover oil from re-X, perform and A/B on it, xtals should appear. A specific kind of mineral spirit being naphtha. acetone or isopropanol then evaporate to collect goods. also acetone is a polar solvent as is IPA and not suitable for extracting from water. if you have too much acetone remaining I would guess the naphtha may I THINK that the more volatile acetone will slowly evaporate from it. The nature of salt plays important role, e. A high pH solution reduces the solubility of DMT. New comments Naphtha is generally cheaper/more easily available, but personally I use naphtha for initial pulls and re x with heptane. Note: I didn't weight the difference. Day 1: Started with 100g ACRB, added 100ml vinegar, basified with 80g pickling lime, put in pie dish, then fridge overnight. Acetone is 0. Hello everyone I've been wondering, would it be viable for someone to use Limonene instead of Naphtha in a STB tek, Lazy Man's, let's suppose? EDIT - This thread has turned more into an acetone extraction question thread, check page 2. 9% freebased at 11. DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO. Would you not get purer/bigger crystals by recrystallizing extracted dmt in acetone? Freebase DMT is very soluble in acetone. Go. More posts you may like r/DMT. Xylene, toluene, and I always amaze myself with making all kinds of mistakes during extraction. Thread Starter Thread You might also consider giving your filter a wash with warm acetone or naphta too and then freeze precip or evaporate. Zippo bought ronsonol and said that they were going to stop using naphtha in the lighter fluid like their own fluid. CONSIDERABLY MORE will evaporate off the resulting extract than naphtha, xylene, toluene or whatever would be able to even under the most optimal conditions. Mimosa is harder to extract than chacruna and chaliponga, so people tend to use sodium hydroxide because it helps break down plant fibers better. Actually better, is to use some acetone or ethanol, redisslve it and re Alternatively use heptane instead of naphtha as DMT is less soluble in cold temperatures in heptane. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? DMT-Nexus, for all your information on DMT Sodium (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO : 02-Dec-2011. Posted : 9/7/2009 5:13:34 PM DMT-Nexus member. solvent used instead of naphtha: Options . If you want to extract DMT N-Oxide as well then use dichloromethane, ether, or chloroform instead of naphtha or heptane. Posted : 6/15/2009 1:16:52 PM DMT-Nexus member. A demijohn could be used instead of the tin below, provided that the bung is removed regularly when heating and shaking, to DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! Visit our NEW FORUM to join the Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » STB » Using Limonene instead of Naphtha in STB. Can I use paint thinner instead of naptha? Extraction It contains 75% naphtha cas 64742-88-7 (marked as medium aliph) and 25% Xylene cas 1330-20-7 If it doesn't leave any rezidue will freezing it still leave a cleaner product? Share You can buy naphtha from eBay A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. B) The solvent mix 1:4 Acetone:Naphtha will not EDIT - This thread has turned more into an acetone extraction question thread, check page 2. The biggest advantage of naphtha is that the solubility of DMT in naphtha is temperature-dependent. Prepare a DMT-saturated solution using either acetone or an NPS ensuring that its container will facilitate the collection of a precipitate and protect the solution from moisture. Can I use acetone as naphtha substitute? Extraction Question/Discussion I can’t get zippo lighter fluid where I live Perfectly white xtals instead of yellowish. Posted SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Bestine would work better for a pull than not heating it up. 7, Acetone Acetone and Naphta are both solvents, Acetone just happens to pull a lot more than the DMT we are looking for. Posts: 6. 3, Ethyl Acetate is 0. i think it might have something to do with the acetone evaporating pretty fast, or the acetone not being dry. crystallizing dmt out of acetone always yielded an oily mess for me that didn't want to crystallize fully. Put all four of your collection jars (containing DMT in a naphtha solution) in the freezer and leave overnight. Lebre #1. 68, and 99. DMT is highly soluble in warm naphtha (up to 50 oC - DMT boils at 67-68 oC) but barely soluble below zero, so the naphtha can be recycled and the precipitate dried rapidly. Posted : 11/22/2008 3:37:21 You put your deem loaded naphtha into Pyrex as usual Then slap it in freezer for 24-48 hrs Then after said time decant (pour off excess naphtha) into another container then fan dry as necessary Will save you a lot of headache DMT-Nexus, for all your information on DMT Sodium (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO : 02-Dec-2011. Members. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. r/DMT. 69ron Rising Star. Stick with xylene, toluene, benzen, ethyl acetate etc. Hello everyone I've been wondering, would it be viable for someone to use Limonene instead of Naphtha in a STB tek, Lazy Man's, let's suppose? SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Bestine would work better for a pull than not heating it up. naptha which evaps rather quickly (hours to a day or two) is a mix of C5-C9 hydrocarbons; the really slow evaporating stuff has toluene, m- and o-xylene, and other aromatics. I would first look up if people have tried it, and their results. Result is highly purified DMT fumarate ready for a second cycle of same. A double boil allows even heat distribution by heating through contact with the water surrounding the jar instead of heating it through contact with the bottom of the pot. [This tendency also depends on the type of plant from which you extracted, and that information may be helpful to include. To answer your question, the primary characteristics that will determine if it's viable will be the associated EDIT - This thread has turned more into an acetone extraction question thread, check page 2. I was following the standard SVG tek instructions (100 g MHRB, 750 ML water, 30 g salt, 100 g lye), had everything all put together and ready to goand my dumb ass grabs the can of Acetone instead of Naptha and dumbs 150 ml of Acetone into my mixture. 1; 2; First Prev 2 of 2 Go to page. one would need to do a m. Thoughts? Locked post. test to confirm this. g. dissolving 2,4 g NaCl in ONE of the 2 samples (ratio retrieved from Max ION TEK) 4. DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts CHAT PRIVACY DONATE: LOGIN REGISTER: FAQ ACTIVE TOPICS: Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » STB » Using Limonene instead of Naphtha in STB. tightly cover the baking dish (id est jars) work better than baking dish for him 3) The naphtha can be poured off quickly and messy or slowly and gently. Extraction Question/Discussion Archived post. When naphtha is added, the DMT transfers into this nonpolar solution layer. We’re a community connected by N,N-Dimethyltryptamine. If the Acetone is not dehydrated (some /all) DMT-Fumarate will stay dissolved in the water. Do not proceed unless you are familiar with handling acetone, 99% IPA, and naphtha. 50 C is at the 74% mark of the liquid range of heptane while -16 C is at the 40% mark of the liquid range of heptane. Sep 9, Now add 50g of ronsonol lighter fluid because you can’t find naphtha to the mixture. Solvent contamination is about the nastiest, but that can generally be taken care of Title is self explanatory SWIM is interested in extracting DMT via straight to base from MHRB. It takes less time and energy to distill it. I’ve seen mixed things about Ronsonol and I have it sitting around at home and was curious if you can use it instead of VM A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. Instead of using a pipette, you want to use EDIT - This thread has turned more into an acetone extraction question thread, check page 2. DMT is 99% freebased at pH 10. EDIT - This thread has turned more into an acetone extraction question thread, check page 2. You can re use it in a later extraction or evaporate it and collect whats left. This xylene was used for the second pull etc etc. FAQ Health and Safety Origins and Development. This helps one avoid residual naphtha. the hardest part is to get the spice out of the jar. It has nothing to do with the DMT. Note: using acetone instead of Naptha or Heptane because it is not accessible to me Note: if this does not work, can I use something else Hi, I've read some posts that say that DMT is highly soluble in Acetone, but I've noticed that nobody ever mentions Acetone in extraction threads or teks, and also nobody mentions it in the many "what can I use instead of naptha" threads; is there a reason for this or would acetone work well as an extraction solvent instead of naptha? 'Round here, acetone is It's more selective for DMT than naphtha and dissolves it very well. Don’t use naphtha or lighter fluid though because it won’t work. Last visit: 03-Jul-2010. Latest reviews Search resources. DMT fumarate is not very soluble in acetone. DMT-Nexus, for all your information on and was wondering: i have some sunnyside (light) naphtha but can easily get some bestine after some research, it appears that defatting has solvent smell, you need to get your spice out of it, and let it air dry for longer. Appearance: Oily forms a SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Bestine would work better for a pull than not heating it up. The FASA Method: DMT Fumarate and Beyond ("FASA" stands for Fumaric Acid Saturated Acetone. Using heptane instead of naphtha? Thread starter azn921; Start date Mar 28, 2012; But, instead of the ammonia wash of the final product, use the sodium carbonate wash from Vovin's Tek Clean naphtha means clean DMT . This powder is about 2 parts chlorophyll to 1 part salvinorin A. instead of naptha would 190 proof (95% grain alcohol, made for oral consumption and cannabis extracts. If not, place it in front of a fan for 5-10 minutes to let some evaporate (thus concentrating the solution) and try again. DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! Visit our NEW FORUM to join the Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » STB » Using Limonene instead of Naphtha in STB. Go for hexane if you can find it, since it is more volatile. Hey guys, just curious as to what would happen if I let 100g of ACRB soak in acetone for 24 hours, filtered and evaped? As I understand it the residue would be a mixture of DMT, plant fats and other impurities. You have to salt out the N,N-DMT, which puts you back at square one if you want the freebase. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? Take your dmt-containing naphtha and put it in a small glass jar. Will it work the same way, or do I have to do something different? My current procedure is cooking my bark with vinegar, basifying with lye, extracting with naphtha 4 times, crashing out crystals in freezer, and if needed 1-3 washes with sodium carbonate. When you freeze precipitate the DMT in heptane or naphtha, the DMT N-Oxide will not dissolve in the solvent and will sink Title pretty much says it all. This tek uses only citric acid, fumaric acid, acetone, sodium carbonate, and water. A basic phase is hydroxanion-rich, and cation-poor (lacks protons), and those hydroxyanions disrupt interactions between acetone and water molecules. New New media New comments Search media. Also the purity of it is often quite questionable. Acetone instead of Naptha for extraction? Options . If it can easily be read otherwise and DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO. Welcome to /r/DMT. Mix it. Acetone and ethanol are incredibly safer to ingest. You will be left with a bright green powder – about 1g per 100g of leaf. Can I use butane instead of naphtha Extraction Question/Discussion Have only done 2 extractions and I’ve found it hard to get naphtha in the uk so I use heptane instead, however I feel like my yields are fairly low Yes, Acetone can potentially be used. how much of dmt can 50g of mimosa powder can make? if i use heptane instead of naphtha, do i it the same with the preheat EDIT - This thread has turned more into an acetone extraction question thread, check page 2. Add your thoughts and get the conversation going. You can't freeze precipitate N,N-DMT freebase from it and you can't evaporate it. Posted : 1/21/2009 12:47:55 AM But neither solvent will extract DMT N-Oxide. (In my defense the two cans look nearly identical). Do not believe the QT tek. Chlorophyll is somewhat soluble in naphtha, salvinorin A is insoluble in naphtha. Still with heptane DMT fumarate is nearly insoluble in acetone, DMT freebase is very soluble in acetone. NPS for FASA Instead of using Aceton as the DMT carrier solution, some non-polar solvents I THINK that the more volatile acetone will slowly evaporate from it. STEP 3: EXTRACTING THE DMT FROM THE NAPHTHA SOLUTION. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? In the end it may even be a solution of Naphtha in DMT) Naphtha (20 °C, C6-C7) 2,93 g in 100 ml Naphtha in the freezer (-20 °C, C6-C7) 109 mg in 100 ml (Fumaric Acid Saturated Acetone) DMT Citrate. If you use pie teks then DMT Extraction Paths. Attitude. tspirit said: - basify water SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Azure Naphtha (search on ebay) or clipper fluid from Poundland. It doesn't pull DMT as efficiently as other solvents, but it's readily available in most countries. The naphtha that is poured out of your dish into a jar could have some DMT in it. Though it requires more careful processing and more thorough wading/cleaning steps. Figured the bark must have oxidated due to age and the naphtha wasn't able to pull dmt-oxide etc. The only reason for ever using naphtha is because it is cheaper. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? Instead it will form a blob then, which looks like this and will settle down immediately instead of having to wait. I don’t know, worth a try! White spirits from B&Q works just fine as a naptha substitute, just don't bother evapping 75% as you will be waiting for weeks, just pop straight into the freezer then once crystals have formed discard the white spirits and plate the crystals in a pyrex dish and leave to evap, will take 2-3 days until there is no smell of white spirits left and the crystals are fully You can probably clean it with a small A B extraction. Acetone can be purchased at hardware stores but should be confirmed as pure acetone prior to purchase. As a general rule-of-thumb with regard to solubilities of alkaloid salts, water>methanol>ethanol>isopropanol>acetone>MEK. 1. SWIM has 99% ISOPROPYL ALCOHOL (IPA)and would like to use it as their Non polar Solvent (instead of Naphtha). Straight and Spiral Router Bits. It To promote harm reduction through open discourse of accurate science in extractions, and the elimination of misinformation about DMT extraction and Ayahuasca brewing. Last visit: 23-Sep-2009 The DMT oil takes a longer to dissolve in hot naphtha. Basically most of the naphthas around are a mixture of short aliphatic hydrocarbons, i. (which is necessary to achieve a good yield). To freeze precipitate DMT in heptane you dissolve the DMT in 50 C heptane (just below the boiling point of DMT making DMT more soluble in the solvent), and freeze at -16 C and it precipitates out. Note, I didn't just ask about acetone, but pure acetone. being that i'm going for freebase couldn't i just do a real good acetone wash, dry, frebase, dry, and go ahead and make my 3 acetone SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Bestine would work better for a pull than not heating it up. 01 atm @ 50C). For every ½ gram of DMT, you will use 50ml of fresh Naphtha or Heptane. (General discussion on the use of DMT & DMT experiences should be posted in r/DMThub) But neither solvent will extract DMT N-Oxide. In order to be utilized for extraction, sodium bicarbonate must undergo conversion to sodium carbonate. Posted : 11/22/2008 3:37:21 There has recently emerged a third option (see the FASA Method) that forgoes the use of water, instead using acetone as the extraction solvent. My question is should I leave the naphtha to fully evaporate for a few days? Thanks Welcome to /r/DMT. ) and lightly shake or stir for 5-10 min then let sit for 2 hours. 4. Thread starter . All-the-sane #1. you can also reuse that naphtha, now that its not up in smoke. As for how you can tell if the acetone has evaporated yet I don't know, but I doubt the extraction is screwed at all. DMT-Nexus Resources. You can freeze precipitate DMT in heptane, and it seems to work better. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? A Safer DMT Extraction - No Lye, No Naphtha For one thing, it inspired a DMT extraction that doesn't require any lye or hydrocarbon solvents (like naphtha, toluene, etc. Anhydrous acetone is needed because mescaline (1:5,,,1ml(or less) naphtha for every 5g mHRb) freezing produces cleaner product as well. e hexane to decane, sometimes entecane and - neither naphtha nor acetone will dissolve dmt-fumarate, so fats/impurities that are pulled into naphtha from the basified water aren't much of an issue And one will get far superior results if the acidic MHRB solution is shimmered/boiled instead of just letting it sit for some time. has anyone had any experiences with heptane instead of naphtha? any noticeable discrepenacies between extractions with the variable being heptane or napthah? any precautions w/ heptane? DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! Visit our Mescaline CIELO TEK DMT salt e-juice HIELO TEK Salvinorin Chilled Acetone with IPA and Naphtha re-X TEK but simply a powder instead of crystals. Last visit: 27-Jul-2009 Hi, I've read some posts that say that DMT is highly soluble in Acetone, but I've noticed that nobody ever mentions Acetone in extraction threads or teks, Dissolve 309 mg of Fumaric acid in another batch of 50 ml of Acetone. has anyone had any experiences Forums. Now add 100ml of the same vinegar/distilled H2O solution. This way you get all the DMT as well as the DMT N-Oxide. 68. This TEK uses freezer chilled acetone to extract salvinorin while minimizing the extraction of other plant material. after all you can just mix bleach and acetone. It may be that you've got all that there is to get and the DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts Mescaline CIELO TEK DMT salt e-juice HIELO TEK Salvinorin Chilled Acetone with IPA and Naphtha re-X TEK The result from sulfuric acid is beautiful too and the xtalization is much faster (30min instead of 24 hours). Naphtha, however, is reported to cause fumaric acid to precipitate out of acetone, disrupting any significant chemical reaction from occurring. NMT freebase should be very soluble in acetone like DMT too, Hexane, heptane or naphtha can likely be substitued for pet ether. 100 mL of acetone can dissolve about 618 mg of fumaric acid) I had no involvement in discovering the methods described below; many thanks go out to Posted by u/subaru_natsuki337 - 1 vote and 6 comments A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. Joined: 14-May-2009. To do this, dissolve the crystals in water and vinegar ph 2-3 and add some naphtha and absorb all the mineral oil residue with the naphtha and discard it afterwards, repeat this 2-4 times, then change the acidic dmt salt solution with sodium hydroxide to ph 12, and continue normally with the extraration as you know it. DCM is 1. Allow acetone to evaporate in a dark, well-ventilated area. I would try putting the mix in as open a container (big glass dish for example) as possible. 6mg of DMT free base per ml of naphtha based on salting results. DMT was scraped and weighted. DMT is moderately soluble in room-temperature naphtha, but barely soluble in ice-cold naphtha. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? Mineral spirits are a broad group of solvent. lots of oils stay in naphtha instead of dried at bottom with dmt. Collect powder, and add about 50mL naphtha per gram, mix well. Note that almost all acetone can contain up to 5% water contamination, depending on time and shelving conditions. I thought of something, being that i'm going for freebase couldn't i just do a real good acetone wash, dry, frebase, dry, and go ahead and make my 3 acetone A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. Then pull with naphtha. I did not find naphthat, but instead picked up this Klean Strip Painter's Solvent - [ Klean-Stripp Painter’s Solvent is a premium, highly refined solvent formula that replaces MEK, Toluene, Xylene and VM&P Naphtha for most applications. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? DMT-Nexus, for all your information on DMT, Ayahuasca and the sorts We've Moved! Visit our NEW FORUM to join the Welcome to the DMT-Nexus » DMT EXTRACTION » DMT Extraction paths » STB » Using Limonene instead of Naphtha in STB. Shop All. I will say that 69ron’s Dlimone tek is meh. Before starting the re-x process, you need to decide how much DMT you will re-x. shrdlu Rising Star. DMT-Succinate (x) DMT-Oxalate (dust instead of real crystals) DMT-Salts that will be a wax (x) DMT Mescaline CIELO TEK DMT salt e-juice HIELO TEK Salvinorin Chilled Acetone with IPA and Naphtha re-X Turns out it still had ~0. DMT-Nexus member. Joined: 16-Jan-2009. Joinery Router Bits Naphtha-NPS good for pulling DMT only, no jungle spice-boiling range 30-200°C (full range naphtha) Water washed away fumaric acid and acetone, leaving back clean xylene (plus the yellowy plant oils that dissolved into it). I've never followed this step. YOUR BODY CAN BREAK THEM Hey people, I'm interested in using d-Limonene isntead of naphtha in an A/B extraction. heating samples to 40 °C and extracting with 1 pull of 25 ml Naphtha for 5 min with a magnetic stirrer Then the Naphtha was separated immediately and evaporated. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? 8/29/2022 Edit: DMT citrate e-juice salt has matured into a TEK. This makes it much safer for the layman than playing with strong lye solutions and being exposed to the vapors of Naphtha-NPS good for pulling DMT only, no jungle spice-boiling range 30-200°C (full range naphtha)-fast evaporation, odor better than toluene/xylene Water washed away fumaric acid and acetone, leaving back clean xylene (plus the yellowy plant oils that dissolved into it). When you freeze precipitate the DMT in heptane or naphtha, the DMT N-Oxide will not dissolve in the solvent and will sink EDIT - This thread has turned more into an acetone extraction question thread, check page 2. He hasn't found any information on it (yet) since most seem to write about the other solvents in their recrystallization process (heptane, naphtha, limonene, etc). In this respect, acetone is useless for pulling spices Acetone is to be used to dissolve magic and infuse herbs. Dried DMT; Naphtha or Heptane; A standard cooking pot A Pyrex casserole dish for freeze precipitating; A beaker or small mason jar; Preparing to re-x. it's nice for making changa however. Posted : 1/21/2009 12:47:55 AM Introduction. But that shouldn't be an issue? Unless acetone is reacting It cannot be separated out just as naphtha, xylene, toluene, DCM hexane, heptane etc separate out when mixed with water. Disregard what they are saying. Then proceed to pull with naphtha as usual in the correct container. SWIM was wondering if one used Bestine/Heptane instead of Naphtha for a pull out of basified water, does one heat up the Bestine just as Naphtha? SWIM knows that Bestine's evap temp is lower than Naphtha so it would probably heat a lot quicker but SWIM was just wondering if heating up the Bestine would work better for a pull than not heating it up. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? EDIT - This thread has turned more into an acetone extraction question thread, check page 2. Can I use chloroform instead of naphtha for a DMT extraction? I saw a procedure on PsychonautWiki but I really don't wanna work with naphtha. If you freebase the DMT, then it's extremely soluble in acetone. Be the first to comment Nobody's responded to this post yet. Pour off and save the solvent, dry, and scrape. What's new. Would one be able to use sodium bicarbonate instead of NaOH in basifying DMT? Back in 2010. (Bi)carbonate instead of NaOH in basifying DMT for an A/B (ALSO ACETONE EXTRACTION NO LYE NO : Options . You'd need to freebase it again and have another solvent that you can evaporate or freeze precipitate from. Posted : 1/21/2009 12:47:55 AM Add your DMT muck to the Naphtha and shake until it's dissolved. With extracting dmt, is heptane better than using naphtha? i read that heptane speeds up the reaction much more than naphtha. Add 500mL of naphtha to the jar and seal it. I am trying Acetone for DMT Extraction . Then follow step 5. wngv mpzmn gjzvc pur hrztmjq msf rhky xcfj enowhd fpfb